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Goal of this procedure: Enter oven mode and reach desired oven profile

Instructions: To keep track of changes to the procedure - copy this page, date it, and add execution notes in red. Remember to save changes.

Table of Contents:

Table of Contents


                    NOTE - WORK IN PROGRESS!

Procedure

Checkout and setup


Procedure Execution notes
1Record goal density and helium buffer pressure

2

Set 10 Torr gauge set points to plus and minus 1 Torr of desired pressure

    • Note: the hysteresis value is where the trip occurs, the lower value is where the fault will clear
 
3Set the 1000 Torr gauge setpoint to 20 Torr

4

Confirm helium gas bottle is connected to fill line 1, regulator set to 5-10 psig 
5If using DPS, confirm it is operating nominally.

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Procedure for oven turn on


Procedure Execution notes
1Verify vacuum conditions approximately 1e-6 Torr or better - Record pressure

2

Zero the 10 and 1000 Torr gauges

 

Purge fill line by running a small amount of He through the fill valve and then stopping and pumping out the IP - Record final pressure
3

Set EPS EXPERT Mode to be “ON” by turning the interlock key in the EPS box in Rack 20-27 in the gallery.

    • Note: EXPERT mode is “OFF” if the LED light is OFF and EXPERT mode is “ON” if the red light is ON)

4Unlock oven gate valves (switch to CAMAC mode) 
5Open oven gate valves 3183 and 3187. (there might be a small amount of helium between the valves). Continue pump down to 1e-6 Torr - Record pressure
6

Close angle valve VV3201 isolating the plasma beamline from the plasma turbo


7Check Beryllium window valve VV3208 is closed- close if not!
8

Set up strip-tool of pressure in the plasma oven:

    • VGCM:LI20:M3201:PMONRAW
    • VGCM:LI20:M3203:PMONRAW

9Fill IP with He to goal IP pressure. If using DPS then follow: How to perform a static fill with DPS
10Hit EPS Reset to clear the low pressure fault
11

Set EPS EXPERT Mode to be “OFF” by turning the interlock key in the EPS box in Rack 20-27 in the gallery. (Note: EXPERT mode is “OFF” if the LED light is OFF and EXPERT mode is “ON” if the red light is ON) . 


12While at the racks, Turn valve control for the beryllium window valve to local only and remove key. Note: the EPICS controls for this valve are also password protected so this will be very well configuration controlled.
13Back at the computer, perform an EPS reset (this is needed to enable the heater)
14

Set up striptool of oven thermocouples plus the thermocouples on the bypass line, cooling water jackets, base-plate and air.

  • Saved as Li_oven_startup.stp

15

Raise heater power (Upstream Heater PS1) slowly (~ 100 Watts per hour) while monitoring the oven pressure and temperature until desired operating conditions and are reached at approximately 550 W (table and plot in next column)- we probably need 10% higher than UCLA to match the profile so don’t be scared to push it up a bit to 600 W. 

  • Will eventually be Epics controlled, but for now it is manual control
  • Multiply the Voltage with Current to get total power - record I, V, P and time.
  • Monitor temperature of bypass. Do not exceed 100 C on viewports. If 100 C is reached, shut down oven following shut down procedure.
      • (I don’t think this ought to be a concern since it has never gone above 50 degrees and if it does, it may just mean the TC is loose and striking the oven).

Notes from March 2022:

  • 29.2*3.33 = 97 W - 10:15 am, 30 deg C
  • Aborted…
  • 29.2*3.33 = 97 W - 11:15 am, 77 deg C
  • 41.7*4.78 = 199 W - 11:40 am, 134 deg C 
  • 52.2*5.95 = 310 W - 12:40 pm, 350 deg C
    • Note: I saw pressure rise from 4.00 to 4.05 Torr coincident with lithium change of state. Ken says lithium is pushing the helium out.
  • Beamline valves fault crash. Recovered. Needed to bypass 3259 and 3291
  • 60.5*6.8 = 410 W - 1:45 pm, 673 deg C
  • 66.8*7.43 = 496 W - 3:00 pm, 538 deg C
  • 72*7.99 = 575 W - 4:00 pm, 768 deg C
16

Check that the oven thermocouple readings are nearly the same as those shown on the profile plot. Ambient conditions may vary, so fine tune the pressure and heater power as needed.

  • Reducing the helium gas pressure in a hot oven could cause loss of lithium. Reduce the heater power to achieve the desired oven temperature then slowly reduce the helium pressure. Slowly raising the buffer gas pressure will not harm the oven.


Procedure for oven shut down

9 hours turning down by hand- 11 hours until valves can be closed


Procedure Execution notes
1

2


 
3

4


 
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Figures:

Li oven sketch with TC locations

Image Modified

Li density profiles

From: Summary of FACET II lithium oven measurements - June 3, 2021

More profiles available in doc (3 Torr, 4 Torr, 6 Torr, 8 Torr