...
- Move MONO to the energy corresponding to the middle of your desired XAS scan energy range.
- This number The ending energy of your XAS scan energy range can be found by going to the Regions window and selecting the scan region you will use. Look towards the bottom of the window for the "stop energy" value.
- Set MONO to the midpoint between your edge energy and the "stop energy" value
- Alternatively, if the scan region is not yet defined, set energy to (edge energy + 500 eV) if you plan to run EXAFS, or (edge energy + 100 eV) if you plan to run only XANES.
- Close S1VGAP to 1.0 mm and S1HGAP to 10.0 mm.
- Scan TABLEVERT motor while looking at I0 signal.
- TABLEVERT scan parameters and apperance depend on mirror cutoff selected
- If at 4 keV cutoff:
- Scan +/- 3.5 mm, with 0.35 mm point spacing (Or use "rel3_5" align region from drop down).
- Select peak slightly to left of center of plateau. Hit "Accept position" Do NOT select peaks at either right or left side of plateau.
- If at 6 keV cutoff:
- Scan +/- 2.5 mm, with 0.25 mm point spacing (Or use "rel2_5" align region from drop down).
- Select peak on right side of scan. Hit "Accept position".
- If at 10 keV cutoff:
- Scan +/- 2.0 mm, with 0.2 mm point spacing (Or use "rel2" align region from drop down).
- Select peak value of I0. Hit "Accept position".
...